烟用香料配制的气相色谱法质量控制研究

采用气相色谱法对香料房卷烟用料液中的溶剂及水分进行检测,分析测定其中的水分、乙醇、丙二醇、山梨醇等的含量,通过对香料房每批配制料液的抽检,可以跟踪料液配制的准确性,保证卷烟产品质量,该方法操作简单、准确性高、重现性好。     

莺歌海盆地CO2成因及运聚特征的初步研究

在已获天然气地地化资料的基础上，重点论述了ＣＯ２天然气地化特征及成因类型，追踪和判识ＣＯ２气烃类气的气源，初步了ＯＣ２气的分布特征及控制因素，指出本区ＣＯ２气属壳源型岩石化学的成因，气源主要来自莺黄组中、下部含钙海相泥岩，与深部火山慢源的ＣＯ２气无关，谱不具深源的特征。     

采用激光光刀的叶片三维面形测量方法

提出一种采用激光光刀的叶片三维面形测量方法。介绍了方法原理、系统结构、信息获取与处理方案,并给出了对实际飞机发动机叶片的面形测量结果。     

SISAK快速化学分离装置的建立

SISAK(Short-lived Isotopes Studies by the AKUFVE technique)技术是目前使用最广泛的快速化学分离方法之一,主要应用在短寿命核素的分离和鉴别、超重元素的人工合成以及化学性质研究等方面的工作中.本文简单地叙述了SISAK技术的流程、原理和发展现状,介绍了自行建立的国内第一套基于SISAK技术的快速化学分离装置,并通过从裂变产物中分离短寿命核素这一实例验证了SISAK技术在快速化学分离中的优越性.     

GC/MS characterization of mate tea leaves extracts obtained from high-pressure CO2 extraction

This work presents a study concerning the chemical characteristics and analytical separation process of the essential oil obtained from high-pressure carbon dioxide extraction of Ilex paraguariensis. The experiments were performed in a laboratory-scale unit in the temperature range of 20–40 °C, from 100 to 250 bar. A blend of the I. paraguariensis extracts was percolated through a preparative chromatographic column, containing silica gel, and successively eluted with 150 mL of each of the following solvents: hexane, toluene, dichloromethane, ethyl acetate, acetone and methanol. The raw extract and its fractions were analyzed by gas chromatography coupled to mass spectrometry detection (GC/MS). The fractionation procedure showed to be a good clean up technique due to the isolation of different classes of compounds in each fraction. Chromatographic analyses allowed the identification of caffeine, fatty acids and esters, phytol, squalene, Vitamin E, stigmasterol derivatives and saturated hydrocarbons.     

Lowering the erosion wear of long blades of the last stages by optimum hanging

Problems of optimum hanging of long rotor blades of the last stages of steam turbines are considered. Causes of nonuniform erosion wear of the inlet edges connected with inaccurate location of holes for the external damper coupling on the chord of the profile are determined. Methods for optimizing the hanging of blades for raising the reliability of the last stages are suggested. Main results of hanging performed with the help of a specially developed “LIBRA” soft hardware are presented. __________ Translated from élektricheskie Stantsii, No. 11, November 2006, pp. 36–41.     

基于一种改进BP网络算法的水轮机组故障诊断

水轮机组状态监测与故障诊断系统,在水轮发电机组及电力系统中有着举足轻重的地位,提高水轮机组状态监测与故障诊断系统的准确性和及时性,对电力系统的安全运行具有重大意义。作者采用一种改进的BP网络算法,用于水轮机组状态监测与故障诊断系统中,试验表明,此方法改善了传统BP网络容易陷入局部最小点、网络收敛速度慢等不利因素,提高了水轮机组状态监测与故障诊断的准确性。     

β放射性气体浓度计的新分度方法

本文介绍β放射性气体浓度计的一种新的分度方法——泄漏元件排气法。其特点是一只元件可分度放射性气体浓度计的许多读出数(甚至是几个量程),操作方便。     

MASS TRANSFER IN GAS-SPARGED POROUS ELECTRODES

The electrochemical limiting current method was used to measure mass transfer coefficients with cocurrent upward gas-liquid flow in packed bed electrodes. Liquid-solid and overall gas-solid coefficients were determined from limiting current data in the presence of inert or reactive gas flows with the use of a plug flow model. The presence of inert gas flow increased mass transfer coefficients over those in single-phase flow by a factor of up to 1.7. As a result of boundary layer penetration by gas bubbles, sparging with reactive gas increased mass transfer rates by a factor of up to 3.5.     

气相起爆系统现场应用试验研究

在现场试验的基础上,对气相起爆系统的实际应用性能进行了初步研究.分析和探讨了该系统安全使用条件和尚存在的诸多技术问题.此外,还介绍了我国首批研制成功的气相雷管及其性能.